Certificado de análisis de muestra
ACS
COA de muestra. Contacte con Alliance Chemical con su número de lote para solicitar un COA específico de ese lote.
Referencia de especificaciones de muestra para Talc Powder ACS. Los resultados del documento fuente son valores de referencia, no mediciones de su lote.
| Parámetro | Especificación | Resultado de referencia del documento fuente | Método de ensayo |
|---|---|---|---|
| Content of magnesium | 17.0 % to 19.5 % | 19.0 % | Atomic absorption spectrophotometry, magnesium emission line 285.2 nm, air-acetylene flame |
| Absence of asbestos | Absence of asbestos; certificate of analysis states the absence of asbestos and the method used | Passes test | IR absorption (test A) or X-ray diffraction (test B); if either is positive, optical microscopy per USP <776> (test C) |
| Acid-soluble substances (as SO4) | 2.5 % max | 0.42 % | — |
| Acidity and alkalinity | Not more than 0.4 mL of 0.01 N hydrochloric acid; not more than 0.3 mL of 0.01 N sodium hydroxide | Passes test | Boil 2.5 g with 50 mL carbon dioxide-free water under reflux; titrate filtrate with bromothymol blue TS and with phenolphthalein TS |
| Free alkali (as NaOH) | 1 % max | 0.028 % | — |
| Arsenic | 3 mg/kg max | 0.40 mg/kg | — |
| Limit of calcium | 0.9 % max | 0.24 % | Atomic absorption spectrophotometry, calcium emission line 422.7 nm, nitrous oxide-acetylene flame |
| Heavy metals | 0.004 % max | 0.00078 % | — |
| Identification A (infrared absorption) | Maxima at 3677 +/- 2 cm-1, 1018 +/- 2 cm-1 and 669 +/- 2 cm-1 | Passes test | IR spectrum of a potassium bromide dispersion |
| Limit of iron | 0.25 % max | 0.064 % | Atomic absorption spectrophotometry, iron emission line 248.3 nm, air-acetylene flame |
| Limit of lead | 0.001 % max | 0.000052 % | Atomic absorption spectrophotometry, lead emission line 217.0 nm, air-acetylene flame |
| Limit of aluminum | 2.0 % max | 0.12 % | Atomic absorption spectrophotometry, aluminum emission line 309.3 nm, nitrous oxide-acetylene flame |
| Loss on drying | 0.5 % max | 0.08 % | — |
| Loss on ignition | 7.0 % max | 4.8 % | USP <733>; ignite about 1 g at 1075 +/- 25 C to constant weight |
| Soluble salts | 0.2 % max | 0.035 % | — |
| Water-soluble substances | 5 mg (0.1 %) max | 1.0 mg | Reflux 10.0 g with 50 mL carbon dioxide-free water 30 min; evaporate 25.0 mL of filtrate, dry at 105 C for 1 hour |
| Identification B (X-ray diffraction) | Diffraction pattern corresponds to that of the talc reference standard | Passes test | XRD, Cu K-alpha, compared to talc reference standard |
| Fineness (residue on 75-um / No. 200 sieve) | 99.0 % min passing | 99.8 % | Dry sieve analysis, 75-um woven-wire sieve |
Los límites de especificación y los resultados del documento fuente se reproducen de la referencia actual del producto utilizada en la ficha técnica. Esta muestra no es un certificado emitido y no identifica un lote analizado. Contacte con Alliance Chemical indicando el producto y el número de lote para obtener documentación específica del lote.
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